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Temperature-dependent structure of an intermetallic ErPd2Si2single crystal: a combined synchrotron and in-house X-ray diffraction study
Sun, Kaitong1,2,3; Zhu, Yinghao1,3; Wu, Si1,3; Xia, Junchao1; Zhou, Pengfei1; Zhao, Qian1; Cao, Chongde4,5; Li, Hai Feng1
2022-04-28
Source PublicationPOWDER DIFFRACTION
ISSN0885-7156
Volume37Issue:2Pages:91-97
Abstract

We have grown intermetallic ErPd2Si2 single crystals employing laser diodes with the floating-zone method. The temperature dependence of the unit-cell parameters was determined using synchrotron and in-house X-ray powder diffraction measurements from 20 to 500 K. The diffraction patterns fit well with the tetragonal I4/mmm space group (No. 139) with two chemical formulae within the unit cell. The synchrotron powder diffraction study shows that the refined unit-cell parameters are a = 4.10320(2) Å, c = 9.88393(5) Å at 298 K and a = 4.11737(2) Å, c = 9.88143(5) Å at 500 K, resulting in the unit-cell volume V = 166.408(1) Å3 (298 K) and 167.517(2) Å3 (500 K). In the whole studied temperature range, no structural phase transition was observed. Upon cooling, the unit-cell parameters a and c are shortened and elongated, respectively.

KeywordErpd2si2 Rietveld Refinement Structure Synchrotron And In-house X-ray Powder Diffraction
DOI10.1017/S0885715622000100
URLView the original
Indexed BySCIE
Language英語English
WOS Research AreaMaterials Science
WOS SubjectMaterials Science, Characterization & Testing
WOS IDWOS:000792224900001
PublisherCambridge University Press
Scopus ID2-s2.0-85129604510
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Document TypeJournal article
CollectionINSTITUTE OF APPLIED PHYSICS AND MATERIALS ENGINEERING
Corresponding AuthorCao, Chongde; Li, Hai Feng
Affiliation1.Joint Key Laboratory of the Ministry of Education, Institute of Applied Physics and Materials Engineering, University of Macau, Taipa, Avenida da Universidade, 999078, Macao
2.State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai, 200050, China
3.Guangdong-Hong Kong-Macao Joint Laboratory for Neutron Scattering Science and Technology, Dongguan, No. 1. Zhongziyuan Road, Dalang, 523803, China
4.Research and Development Institute, Northwestern Polytechnical University in Shenzhen, Shenzhen, 518057, China
5.School of Physical Science and Technology, Northwestern Polytechnical University, Xi'an, 710072, China
First Author AffilicationINSTITUTE OF APPLIED PHYSICS AND MATERIALS ENGINEERING
Corresponding Author AffilicationINSTITUTE OF APPLIED PHYSICS AND MATERIALS ENGINEERING
Recommended Citation
GB/T 7714
Sun, Kaitong,Zhu, Yinghao,Wu, Si,et al. Temperature-dependent structure of an intermetallic ErPd2Si2single crystal: a combined synchrotron and in-house X-ray diffraction study[J]. POWDER DIFFRACTION, 2022, 37(2), 91-97.
APA Sun, Kaitong., Zhu, Yinghao., Wu, Si., Xia, Junchao., Zhou, Pengfei., Zhao, Qian., Cao, Chongde., & Li, Hai Feng (2022). Temperature-dependent structure of an intermetallic ErPd2Si2single crystal: a combined synchrotron and in-house X-ray diffraction study. POWDER DIFFRACTION, 37(2), 91-97.
MLA Sun, Kaitong,et al."Temperature-dependent structure of an intermetallic ErPd2Si2single crystal: a combined synchrotron and in-house X-ray diffraction study".POWDER DIFFRACTION 37.2(2022):91-97.
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