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Residual stress measurement in textured thin film by grazing-incidence X-ray diffraction
Ma C.-H.2; Huang J.-H.1; Chen H.2
2002-10-15
Source PublicationThin Solid Films
ISSN00406090
Volume418Issue:2Pages:73-78
Abstract

Measurements of residual stresses in textured thin films have always been problematic. In this article, a new experimental method using grazing-incidence X-ray diffraction is presented with its principles based upon the conventional sin ψ method. Instead of using the Bragg-Brentano (B-B) or Seemann-Bohlin geometry, the proposed method utilizes an asymmetrical diffraction geometry for which the X-ray beam is incident at a grazing angle γ to the sample surface, while the angle ψ is the tilt angle of the sample surface as defined by the conventional sin ψ method. Basic equations involved in the X-ray residual stress analysis are described, along with exemplified experimental data. Analysis shows that, for an isotropic medium, strain measured using this grazing-incidence geometry assumes a linear relationship with the geometrical parameter cos α sin ψ, where the angle α is a constant and is defined as the Bragg angle at ψ = 0°, θ , minus the grazing incidence angle γ, i.e. α = θ -γ. The grazing-incidence diffraction geometry effectively increases the irradiation volume from a thin-film specimen, thereby giving rise to higher intensity for high-angle Bragg peaks than the conventional B-B geometry. The proposed analysis has another advantage, in that the inhomogeneous sample casts little effect on the residual stress results when compared to the traditional sin ψ method. © 2002 Elsevier Science B.V. All rights reserved.

KeywordCos 2 α Sin 2 ψ Method Residual Stress Textured Thin Film
DOI10.1016/S0040-6090(02)00680-6
URLView the original
Language英語English
WOS IDWOS:000178997600002
Scopus ID2-s2.0-0037109204
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Citation statistics
Document TypeJournal article
CollectionUniversity of Macau
Affiliation1.National Tsing Hua University
2.University of Illinois at Urbana-Champaign
Recommended Citation
GB/T 7714
Ma C.-H.,Huang J.-H.,Chen H.. Residual stress measurement in textured thin film by grazing-incidence X-ray diffraction[J]. Thin Solid Films, 2002, 418(2), 73-78.
APA Ma C.-H.., Huang J.-H.., & Chen H. (2002). Residual stress measurement in textured thin film by grazing-incidence X-ray diffraction. Thin Solid Films, 418(2), 73-78.
MLA Ma C.-H.,et al."Residual stress measurement in textured thin film by grazing-incidence X-ray diffraction".Thin Solid Films 418.2(2002):73-78.
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