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Synthesis and characterization of large single crystal of ZAPSO-43
Xu X.T.3; Zhai J.P.3; Chen Y.P.3; Li I.L.3; Chen H.Y.1; Ruan S.C.3; Tang Z.K.2
2014-09-15
Source PublicationMicroporous and Mesoporous Materials
ISSN13871811
Volume196Pages:314-320
Abstract

We investigated the effects of gel composition and crystallization conditions on the hydrothermal synthesis of ZAPSO-43 single crystals in detail. Large single crystals of ZAPSO-43 (around 250 μm) with high quality were synthesized by optimizing the following synthesis conditions: crystallization temperature and duration, molar ratio of SiO /Al O and ZnO/Al O , content of HF acid and organic template dipropylamine (DPA). Single-crystal X-ray diffraction measurement show that the as-synthesized ZAPSO-43 are of Fddd symmetry with lattice constants a = 9.9985 Å, b = 14.2565 Å and c = 14.5726 Å, α = β = γ = 90° and their unit volume is V = 2077.22 Å . © 2014 Elsevier Inc. All rights reserved.

KeywordDipropylamine Large Single Crystal Zapso-43
DOI10.1016/j.micromeso.2014.05.042
URLView the original
Language英語English
WOS IDWOS:000340333400038
Scopus ID2-s2.0-84902591069
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Citation statistics
Document TypeJournal article
CollectionUniversity of Macau
Affiliation1.Taishan Medical University
2.Hong Kong University of Science and Technology
3.Shenzhen University
Recommended Citation
GB/T 7714
Xu X.T.,Zhai J.P.,Chen Y.P.,et al. Synthesis and characterization of large single crystal of ZAPSO-43[J]. Microporous and Mesoporous Materials, 2014, 196, 314-320.
APA Xu X.T.., Zhai J.P.., Chen Y.P.., Li I.L.., Chen H.Y.., Ruan S.C.., & Tang Z.K. (2014). Synthesis and characterization of large single crystal of ZAPSO-43. Microporous and Mesoporous Materials, 196, 314-320.
MLA Xu X.T.,et al."Synthesis and characterization of large single crystal of ZAPSO-43".Microporous and Mesoporous Materials 196(2014):314-320.
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